Mini Chemical Reactor Computerized

PIGNAT Mini Chemical Reactor Computerized – REA3000

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SKU: REA3000 Category: Chemical Processes Tags: Chemical, Reactors

Description

Description

Provides a small volume reactor (1 liter) for studying chemical reactions with various parameters

Perform a reaction:

Controlling the temperature of the reaction mixture
Controlling the temperature of the heat transfer fluid
Influencing of stirring speed

Add reagent at the beginning or at a later stage

Reaction media

Homogeneous liquid
Gas-liquid heterogeneous

Proposed Experiments:

Perform organic synthesis (e.g. synthesis of aspirin)
- Study the chemical reaction mechanism and reagent preparation
- Adjust process parameters: temperature, stirring, reagent feed mode
- Aspirin obtained in solvent phase
- Controlled crystallization of aspirin
- Isolate the product, calculate the yield and analyse the purity.

Technical Description:

Reactor:
- Glass tank, double jacket, 1 liter.
- Torion type drainig valve.
- Glass cover.
- Tap for Pt 100Ω Pt temperature probe.
- Nozzle to the glass condenser.
- Glass condenser with an internal coil.
- Glass reagent feed funnel, 500 ml, draining valve
Temperature control unit:
- Electronic display and control of the bath temperature and of the temperature by an external probe (reaction medium).
- Temperature : 20°C to 150°C.
- Heating power : 2000 W.
- Group volume: about 4 L.
- Water cooling
Stirring:
- Adjustable speed motor 0 to 500 rpm.
- Stirring bearing.
- PTFE shaft and mobile.
Cooling water feed :
- Isolating valve.
- Setting valve.
- Float type flow meter.
- Collecting by gravity.
Gas intake circuit :
- Isolating valve.
- Setting valve.
- Float type flow meter.
- PTFE flexible and nozzle.
- Vent above the condenser.

Optional Equipment:

Reactor for internal cooling
- Addition of a glass coil inside the reactor for cooling.
- Selection three way valve for water feed

General Specifications

Glass reactor, jacketed, glass cover, reflux head with distillation valve.
Stirrer, SS/PTFE shaft and mobile.
Glass coil condenser, jacketed.
Glass reagent feed funnel, draining valve and filling hole.
Heating group.

Instrumentation

5 temperature probes Pt100Ω.
Air flowmeter.
Water flowmeter.

Dim : 120 x 55 x 125 cm – 70 kg
SS framework 30 x 30mm

For a complete product data sheet and a list of reference sites please call 1-877-967-2726.

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École Polytechnique de Montreal

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Sheridan College

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University of Toronto

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Kativik School Board

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University of Waterloo

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University of Guelph

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SAIT Polytechnic

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Director, Teaching Labs

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